| 17 Mar 21 | r16  | LaferrereLaferrere | 0 - 2 | San TelmoSan Telmo |
| 17 Mar 21 | r16 | ColonColon | 0 - 1 | Argentinos JuniorsArgentinos Ju |
| 24 Mar 21 | r16 | Boca JuniorsBoca Juniors | 3 - 0 | Defensores de BelgranoDefensores de |
| 25 Mar 21 | r16 | San LorenzoSan Lorenzo | 0 - 2 | Defensa y JusticiaDefensa y Jus |
| 07 Apr 21 | r16 | Patronato de ParanaPatronato de | 2 - 2 | LanusLanus |
| 07 Apr 21 | r16 | Talleres de CordobaTalleres de C | 1 - 1 | Velez SarsfieldVelez Sarsfie |
| 08 Apr 21 | r16 | Atletico TucumanAtletico Tucu | 1 - 2 | River PlateRiver Plate |
| 15 Apr 21 | r16 | San Martin San JuanSan Martin Sa | 2 - 2 | Racing ClubRacing Club |
| 13 May 21 | r16 | Boca UnidosBoca Unidos | 0 - 2 | Godoy CruzGodoy Cruz |
| 17 May 21 | r16 | Newells Old BoysNewells Old B | 0 - 1 | SarmientoSarmiento |
| 13 Jul 21 | r16 | Club Atlético Villa San CClub Atlético | 0 - 1 | Patronato de ParanaPatronato de |
| 14 Jul 21 | r16  | San TelmoSan Telmo | 1 - 0 | BanfieldBanfield |
| 20 Jul 21 | r16 | SarmientoSarmiento | 0 - 1 | TemperleyTemperley |
| 04 Aug 21 | r16 | TigreTigre | 2 - 1 | IndependienteIndependiente |
| 04 Aug 21 | r16 | Boca JuniorsBoca Juniors | 0 - 0 | River PlateRiver Plate |
| 12 Aug 21 | r16 | Estudiantes de Río CuartoEstudiantes d | 1 - 1 | Talleres de CordobaTalleres de C |
| 18 Aug 21 | r16  | Gimnasia LPGimnasia LP | 2 - 3 | Argentinos JuniorsArgentinos Ju |
| 09 Sep 21 | r16 | Defensa y JusticiaDefensa y Jus | 0 - 0 | TigreTigre |
| 22 Sep 21 | r16 | Godoy CruzGodoy Cruz | 3 - 3 | Racing ClubRacing Club |
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